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Am. J. Enol. Vitic. 49:1:100-104 (1998)
Copyright © 1998 by the American Society for Enology and Viticulture.
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Fast Screening Method for Wine Headspace Compounds Using Solid-Phase Microextraction (SPME) and Capillary GC Technique

Gy. Vas 1, K. Kõteleky 1, M. Farkas 1, A. Dobó 2, and K. Vékey 2

1 Research Institute for Viticulture & Enology of Agricultural Ministry, Eger, Hungary
2 Central Research Institute for Chemistry of the Hungarian Academy of Sciences, Budapest, Hungary.

H12232vas{at}ella.hu

Solid-phase microextraction (SPME) coupled to capillary gas chromatography-mass spectrometry (GC-MS) was used for determination of volatile wine components. This combination offers a simple, quick, and sensitive approach suitable for characterization of wine aroma compounds without a complicated sample preparation procedure. Wines are characterized by "aromagrams", a set of identified components with corresponding relative abundances. Reproducibility (RSD errors of relative peak abundances) due to the analytical procedure are ca. 4%; variations among different samples of the same type of wine from the same region are ca. 8%. SPME-GC(-MS) has been shown to yield far larger differences among different wine types (Chardonnay, Muscat Ottonel, and Tramini) and among the same type of wine produced in different regions, showing the utility of the technique in wine analysis.

Key words: solid-phase microextraction, wine headspace compounds, capillary gas chromatography, GCMS

Submitted on July 15, 1996




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K. L. Howard, J. H. Mike, and R. Riesen
Validation of a Solid-Phase Microextraction Method for Headspace Analysis of Wine Aroma Components
Am. J. Enol. Vitic., March 1, 2005; 56(1): 37 - 45.
[Abstract] [Full Text] [PDF]




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Copyright © 1998 by the American Society for Enology and Viticulture.