PT - JOURNAL ARTICLE AU - P. Fantozzi AU - G. Montedoro TI - Determination of free Amino Acids in Musts and Wines by Gas-Liquid Chromatography AID - 10.5344/ajev.1974.25.3.151 DP - 1974 Jan 01 TA - American Journal of Enology and Viticulture PG - 151--156 VI - 25 IP - 3 4099 - http://www.ajevonline.org/content/25/3/151.short 4100 - http://www.ajevonline.org/content/25/3/151.full SO - Am J Enol Vitic.1974 Jan 01; 25 AB - A method was devised utilizing gas-liquid chromatography (GLC) for qualitative and quantative analysis of 21 free amino acids in musts and wines. The amino acids were analyzed following extraction by ion-exchange resins, silylating dried eluate with N,O-bis (trimethylsilyl) acetamide (BSA), and separation by GLC of their trimethylsilyl derivatives. The results of the GLC carried out in musts and wines were in good agreement with classical ion-exchange amino acid analysis and direct colorimetric analysis of proline. The GLC technnique is sensitive, precise, accurate, and rapid.