@article {Whiton60, author = {R. S. Whiton and B. W. Zoecklein}, title = {Determination of Ethyl Carbamate in Wine by Solid-Phase Microextraction and Gas Chromatography/Mass Spectrometry}, volume = {53}, number = {1}, pages = {60--63}, year = {2002}, doi = {10.5344/ajev.2002.53.1.60}, publisher = {American Journal of Enology and Viticulture}, abstract = {A method for the rapid determination of ethyl carbamate in wine by headspace solid-phase microextraction with detection by gas chromatography/mass spectrometry has been developed. The analysis parameters of fiber coating, extraction time, and sample temperature have been optimized. The optimized method of headspace sampling with a Carbowax/divinylbenzene fiber for 30 minutes has been found to be reproducible and linear from 10 to 80 {\textmu}g/L, with a limit of detection of 9.6 {\textmu}g/L. The method is simple, requires little operator effort, and can be automated.}, issn = {0002-9254}, URL = {https://www.ajevonline.org/content/53/1/60}, eprint = {https://www.ajevonline.org/content/53/1/60.full.pdf}, journal = {American Journal of Enology and Viticulture} }