Determination of free amino acids in wine by HPLC

EM Sanders, CS Ough - American journal of enology and …, 1985 - Am Soc Enol Viticulture
A method of analysis is presented which separates 20 derivatized amino acids in under 35
minutes. Prior to derivatization, white wine samples from a fermentation temperature study …

Determination of amines and amino acids in wine—a review

P Lehtonen - American Journal of Enology and Viticulture, 1996 - Am Soc Enol Viticulture
The significance of amines and amino acids in wine, and the most recent techniques for their
determination and quantification, are summarized. Liquid chromatography is by far the most …

Determination of free amino acids in wine by HPLC using precolumn derivatization with phenylisothiocyanate

RM Marcé, M Calull, J Guasch… - American journal of …, 1989 - Am Soc Enol Viticulture
An analytical method for the determination of free amino acids in wines is reported. It is
based on their transformation into phenylthiocarbamyl derivatives. The derivatives were …

Rapid determination of primary amino acids in grape juice using an o-phthaldialdehyde/N-acetyl-L-cysteine spectrophotometric assay

BC Dukes, CE Butzke - American Journal of Enology and …, 1998 - Am Soc Enol Viticulture
Low levels of yeast assimilable nitrogenous compounds (YANC) in grape juice have been
associated with sluggish or stuck fermentations. In contrast, excessive levels may lead to the …

Determination of amino acids in wort and beer by reverse-phase high-performance liquid chromatography

H Garza-Ulloa, RG Cantú, AMC Gajá - Journal of the American …, 1986 - Taylor & Francis
An analysis of 19 amino acids in wort or beer was based on the precipitation of proteins
followed by precolumn derivatization of the amino acids with o-phthaldialdehyde/2 …

Amino acid determination in musts and wines by HPLC after derivatization with phenylisothiocyanate

PH Orte, A Guitart, J Cacho - American journal of enology …, 1997 - Am Soc Enol Viticulture
The present paper deals with the application of the pre-column derivatization procedure with
PITC to the determination of amino acids levels in must and wine by reverse-phase HPLC …

Identification and determination of amino acid ethyl esters in wines by capillary gas chromatography-mass spectrometry

T Herraiz, CS Ough - Journal of agricultural and Food Chemistry, 1992 - ACS Publications
Method A. Four hundred milliliters of the wine to be analyzed was adjusted to pH 4.5 with 1.5
M NaOH and passed slowly down a cation-exchange resin column (70X 16.5 mm) of …

Rapid HPLC analysis of amino acids and biogenic amines in wines during fermentation and evaluation of matrix effect

YQ Wang, DQ Ye, BQ Zhu, GF Wu, CQ Duan - Food chemistry, 2014 - Elsevier
A rapid HPLC method has been developed for the simultaneous determination of 23 amino
acids, 10 biogenic amines and the ammonium ion in wine. Samples were pre-column …

[CITATION][C] The free amino acids of musts and wines. I. Microbiological estimation of fourteen amino acids in California grape musts

JGB Castor - Journal of Food Science, 1953 - Wiley Online Library
Present knowledge indicates that amino acids may be of basic importance in the production,
flavor, and quality of fermented beverages. However, the literature contains no information …

Use of high-performance liquid chromatography for the determination of amino acids in sparkling wines

A Casoli, O Colagrande - American Journal of Enology and …, 1982 - Am Soc Enol Viticulture
An analytical method is reported that can be used for the determination of amino acids in
sparkling wines based on their transformation into dansyl derivatives and their separation by …