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Research Note

Permeation of d5-2,4,6-Trichloroanisole via Vapor Phase through Different Closures into Wine Bottles

Paulo Lopes, Juliana Marques, Tânia Lopes, José Lino, Joaquim Coelho, Cátia Alves, Isabel Roseira, Adélio Mendes, Miguel Cabral
Am J Enol Vitic. June 2011 62: 245-249; published ahead of print February 23, 2011 ; DOI: 10.5344/ajev.2010.10098
Paulo Lopes
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  • For correspondence: pdl@net.sapo.pt
Juliana Marques
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Tânia Lopes
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José Lino
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Joaquim Coelho
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Cátia Alves
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Isabel Roseira
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Adélio Mendes
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Miguel Cabral
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Abstract

This study examined the sealing effectiveness of different closures on the permeation of exogenous compounds when bottled wine model solutions were stored in a contaminated environment with deuterium-labeled 2,4,6-trichloroanisole (d5-TCA). Wine model solutions and closure fractions (outer, middle, and inner) were assessed over time for the concentration of releasable d5-TCA by SPME-GC-MS. During 24 months of storage, high concentrations of d5-TCA were essentially retained in the outer portions of natural and microagglomerate corks. Under the conditions of this experiment, the natural and microagglomerate cork stoppers were effective barriers to the transmission of exogenous contaminants. Conversely, d5-TCA penetrated synthetic closures and contaminated the wine.

  • trichloroanisole
  • cork stoppers
  • synthetic closures
  • contaminated atmosphere
  • © 2011 by the American Society for Enology and Viticulture
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Permeation of d5-2,4,6-Trichloroanisole via Vapor Phase through Different Closures into Wine Bottles
Paulo Lopes, Juliana Marques, Tânia Lopes, José Lino, Joaquim Coelho, Cátia Alves, Isabel Roseira, Adélio Mendes, Miguel Cabral
Am J Enol Vitic.  June 2011  62: 245-249;  published ahead of print February 23, 2011 ; DOI: 10.5344/ajev.2010.10098

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Permeation of d5-2,4,6-Trichloroanisole via Vapor Phase through Different Closures into Wine Bottles
Paulo Lopes, Juliana Marques, Tânia Lopes, José Lino, Joaquim Coelho, Cátia Alves, Isabel Roseira, Adélio Mendes, Miguel Cabral
Am J Enol Vitic.  June 2011  62: 245-249;  published ahead of print February 23, 2011 ; DOI: 10.5344/ajev.2010.10098
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